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The submicro phase morphology of PS/PP binary polymer alloy is studied. The samples used are prepared by the same way as before. The results are similar to those presented in literatures. But it has been noted that there are some insoluble gels in the alloy when PS/PP with the ratio over 90/10 is dissolved by methylbenzene. Further experiments show that some large disperse phase particles occur in the alloy, but not reported in literatures.
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